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Optimierung der Goniometrie zur Texturbestimmung aus Rntgenbeugungsbildern

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Springer Nature
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N/A
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GTIN
9783658149413
Condition
New
Product Description

Florian Bachmann entwickelt Verfahren zur nutzergesttzten und (teil-)automatisierten Polfigurmessung mit Allzweckdiffraktometern. Fr beliebige Flchendetektoren, Wellenlngen und ein- oder mehrphasige Probenkrper formuliert er die Erzeugung von Messschemata als ein Mengenzerlegungsproblem, das die Anzahl von Messungen minimiert, aber die Abdeckung abzutastender Polsphren maximiert. Hierzu erlutert er die Beugungsgeometrie und schlgt eine Konstruktionsvorschrift fr entsprechende Messraster vor. Die Verarbeitung aufgenommener Rntgenbeugungsbilder zu Polfiguren wird aus dem kinematischen Beugungsmodell abgeleitet und ein angepasstes Verfahren zur Schtzung der Orientierungsdichte besprochen. Zur Automatisierung des Messablaufes erlutert der Autor schlielich Verfahren zur Schtzung bentigter Parameter aus einer initialen Messung und diskutiert anhand von Beispielen die resultierende Optimierung der Goniometrie.

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